Διαθλασίμετρο ακτίνων Χ (XRD)

PANalytical X’Pert PRO MPD

PANalytical
PANalytical X’Pert PRO MPD X-ray Diffractometer (XRD)

Excerpt from the service report:
Device: PANalytical X’Pert PRO MPD
Date: 07/07/2021
Performed works:
- Reinstallation and commissioning of the system
- Connection of external supply lines
- Warm-up phase
- Complete alignment of goniometer and additional components
- Maintenance carried out incl. replacement of defective parts
Spare parts used:
L 3.6V NC/U3 R15.0X52.0 BATTERY. NI-CD
FAN FOR X-CELERATOR UNIT FAN
FILTER FILTER, WATER
Motor PW3050
(Note: “Device not tested at our facility”)

The X’Pert PRO MPD is a highly versatile and powerful X-ray diffractometer (XRD) for the structural characterization of crystalline materials. Perfect for pure research as well as for routine applications in industry and academia. Thanks to its modular design, rapid detection, and temperature and atmosphere control, it is ideally suited for both routine analyses and complex in-situ experiments.

Key features:
Various measurement geometries are possible:
- Reflection in Bragg-Brentano (θ–2θ) mode
- Transmission geometry for powders in capillaries
- Optionally also SAXS (Small-Angle X-ray Scattering) for nanostructures

Radiation source and detectors:
- Usually copper anode (Cu-Kα, λ ≈ 1.54 Å)
- X’Celerator detector (1D, ultra-fast) for parallel data acquisition

Modular system with PreFIX technology:
- Fast exchange of optics and sample stages without recalibration

In-situ measurements at high temperatures:
- Measurements possible up to approx. 1200°C
- Controlled atmosphere: air, nitrogen, oxygen (limited for reducing atmosphere)

Typical applications:
- Phase analysis and quantitative Rietveld evaluation
- Determination of crystallite size, microstrain, residual stresses
- In-situ investigation of phase transitions, oxidation, crystallization, etc.
- SAXS measurements for analysis of nanoparticles and pore structures
- Wide sample spectrum: powders, thin films, ceramics, pharmaceuticals, catalysts, and more

Technical data (typical):
Property & Specification
Angular range (2θ): approx. 0.5° to 150°
Step size: up to 0.002° or finer
Goniometer: vertical, 0–0, radius approx. 240 mm
Temperature range: room temperature up to approx. 1200 °C
Atmosphere: air, N₂, O₂ (limited reducing atmosphere)
Detectors: X’Celerator (1D), proportional counter

Distribution & fields of application:
The X’Pert PRO MPD is in use worldwide, e.g. at:
- Universities (ETH Zurich, TU Dresden, University of Vienna)
- Research institutes (e.g. Max Planck Institutes, ICN2, IS2M)
Dkedpjwycatjfx Aaceu
- Industry (e.g. materials development, pharma, chemistry)

Condition: used
Scope of delivery: (see image)
(Specifications and technical details are subject to change and error!)

If you have further questions, we will be happy to answer them by phone.

Η διαφήμιση μεταφράστηκε αυτόματα και ενδέχεται να περιέχει ορισμένα σφάλματα μετάφρασης.